X-ray powder diffractometer Rigaku SmartLab 3kW (RIGAKU3)


Guarantor:
Pavla Roupcová, Ph.D.

Instrument status:
Some Issues Some Issues, 27.3.2024 15:00, I wanted to bring to your attention an issue encountered during my measurements on Saturday, March 23, 2024. Specifically, I encountered a problem with the optics alignment procedure conducted using the (Package_General Medium resolution PB/PSA (with PB slit)). Regrettably, the operation did not yield the expected optic alignment, and an error message indicated that the optic alignment process had failed. However, upon attempting the optics alignment using an alternative method (PackageGeneral Bragg-Brantor FocusingD/tex), the process was completed successfully.

Equipment placement:
CEITEC Nano - A1.16

Upcoming trainings:
4.4. 13:00 - 17:00: Rigaku3-základní - Bring your typical sample. A1.15 Go through: https://cfmoodle.ceitec.vutbr.cz/mod/lesson/view.php?id=429 https://cfmoodle.ceitec.vutbr.cz/mod/lesson/view.php?id=444


X-Ray Powder Diffractometer equipped with Goebble mirror for HR spectra acquisition and JCPDS diffraction data database. In order to be able to observe temperature-dependent processes, a high temperature and low temperature chambers are planned as parts of the system.


Publications:

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Photogallery

Specification

Radiationfine focus Cu sealed tube; 40kV, 30mA
Goniometerθ/θ or θs, θd independent optical encoder controlled
radius 300 mm
Eulerian craddle (φ, Ω)
Incident opticsCBO, automatic variable divergence slit (BB, PB)
Ge 2-bounce and 4-bounce monochromators
Receiving opticsPSA, Ge 2-bounce analyzer, automatic receiving slit
Detectorsproportional and linear (D-tex)
HTK-16N chamberup to 800°C; vacuum, air, inert gases
TTK 450 chamberdown to –193°C; vacuum, dry gases
XRK 900 chamberup to 900°C, various gases



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