CEITEC Nano Research Infrastructure
Brno University of Technology
Purkyňova 123, 612 00 Brno
Czech Republic
+420 54114 9207
nano@ceitec.vutbr.cz
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Surface area and pore Size Analyzer (3P Micro 300C1, 3P Instruments) (BET-ANAMET)
Guarantor:
Kateřina Tmejová, Ph.D.
Instrument status:
Operational, 4.9.2024 15:08, Record 1
Equipment placement:
CEITEC Nano - B1.14
The instrument includes fully automated volumetric sorption analyzers for measuring adsorption and desorption of nitrogen and other non-corrosive gases on three independent analysis stations. C/C1 version is equipped with micropore stations.
Publications:
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GHOSH, K.; NG, S.; LAZAR, P.; KANDAMBATH PADINJAREVEETIL, A.; MICHALIČKA, J.; PUMERA, M., 2024: 2D Germanane-MXene Heterostructures for Cations Intercalation in Energy Storage Applications. ADVANCED FUNCTIONAL MATERIALS , doi: 10.1002/adfm.202308793; FULL TEXT
(RIGAKU3, KRATOS-XPS, WITEC-RAMAN, TITAN, VERIOS, KEITHLEY-4200, MPS150, BET-DEGASSER, BET-ANAMET) -
ULLATTIL, S.; PUMERA, M., 2023: Light-Powered Self-Adaptive Mesostructured Microrobots for Simultaneous Microplastics Trapping and Fragmentation via in situ Surface Morphing. SMALL , doi: 10.1002/smll.202301467; FULL TEXT
(VERIOS, RIGAKU3, KRATOS-XPS, BET-ANAMET) -
SONIGARA, K.; VAGHASIYA, J.; MAYORGA-MARTINEZ, C.; PUMERA, M., 2023: Flexible energy storage patch based on NiPS3/graphene zinc-ion hybrid supercapacitor for integrated biosensors. CHEMICAL ENGINEERING JOURNAL 473, doi: 10.1016/j.cej.2023.145204; FULL TEXT
(BET-ANAMET) -
Koribanich, I.; Mudra, E. ;Shepa, I.; Hrubovcakova, M.; Kovalcikova, A.; Girman, V.; Pavlinak, D.; Balaz, M.; Dusza, J., 2023: Graphene-coated alumina nano/microfibers as filler for composites. CERAMICS INTERNATIONAL 49(14), p. 24216 - 7, doi: 10.1016/j.ceramint.2022.09.237; FULL TEXT
(KRATOS-XPS, BET-ANAMET) -
TINOCO NAVARRO, L.; CIHLÁŘ, J.; MICHALIČKA, J.; KAŠTYL, J.; ČÁSTKOVÁ, K., 2023: Effect of MCAA Synthesis and Calcination Temperature on Heterojunction Formation and Photocatalytic Activity of Biphasic TiO2 (B/A). CATALYSIS LETTERS 2, doi: 10.1007/s10562-023-04489-7; FULL TEXT
(RIGAKU3, WITEC-RAMAN, FTIR, VERIOS, TITAN, KRATOS-XPS, BET-DEGASSER, BET-ANAMET, ZETASIZER)
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TINOCO NAVARRO, L.; BEDNAŘÍKOVÁ, V.; KAŠTYL, J.; CIHLÁŘ, J., 2023: Structure and Photocatalytic Properties of Ni-, Co-, Cu-, and Fe-Doped TiO2 Aerogels. GELS 9(5), p. 1 - 21, doi: 10.3390/gels9050357; FULL TEXT
(RIGAKU3, VERIOS, BET-ANAMET, JASCO, MIRA-STAN, TITAN)
Photogallery
Specification
The instrument includes fully automated volumetric sorption analyzers for measuring the adsorption and desorption of nitrogen (S1 and S2 station) and other non-corrosive gases (argon – station S3) on three independent analysis stations. The C/C1 version is equipped with micropore stations. Each analysis station has its own dosing manifold for optimal analysis duration. The instrument allows to measure: Single-/Multipoint-BET surface area, Langmuir surface area, Adsorption and desorption isotherms, Total pore volume and average pore radius, NLDFT (density functional theory), Mesopore size distribution according to BJH (DIN 66134) and DH method, Micropore analysis (DIN 66135) according to t-plot, Dubinin-Radushkevich, Horvath-Kawazoe, and Saito-Foley method.
Parameters
| No. of analysis/ pretreatment station | 3 |
|---|---|
| Pressure sensor (P0) | 3x 1000 torr |
| Pressure sensor (analysis station) | 1000 torr 10 torr 1 torr (or 0.1 torrs) |
| Pretreatment temperature | Ambient to 400 °C |
| Temperature | 15 – 35 °C |
| Humidity | 20 – 80 % (non-condensing) |
Specific surface area and sample quantity
| BET/(m2/g) | 0.1~0.5 | 0.5~1 | 1~3 | 3~5 | 5~10 | 10~50 | 50~100 | ≥100 |
|---|---|---|---|---|---|---|---|---|
| Mass of sample (g) | 6~10 | 4~6 | 3~4 | 2~3 | 1~2 | 0.5~1 | 0.2~0.5 | 0.1~0.2 |
Documents
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