Scanning electron microscope (SEM) MIRA3 XMU (MIRA-STAN)
Guarantor:
Petr Lepcio, Ph.D.
Instrument status:
Some Issues, 10.12.2024 22:36, RBSE calibration error
Equipment placement:
CEITEC Nano - A1.11
Upcoming trainings:
23.1. 09:00 - 15:00:
MIRA-STAN 1/2 -
Meeting point at the microscope. This is a two-step training, register for part 2 in our booking system. Obligatory prerequisites must be completed 2 days before the training. More information about the training is available on our <a href=”https://cfmoodle.ceitec.vutbr.cz/course/view.php?id=76”>Moodle</a>.
28.1. 09:00 - 12:00:
MIRA-STAN 2/2 -
Meeting point at the microscope. This is a two-step training, register for part 1 in our booking system. More information about the training is available on our <a href=”https://cfmoodle.ceitec.vutbr.cz/course/view.php?id=76”>Moodle</a>.
30.1. 09:00 - 12:00:
MIRA-STAN 2/2 -
Meeting point at the microscope. This is a two-step training, register for part 1 in our booking system. More information about the training is available on our <a href=”https://cfmoodle.ceitec.vutbr.cz/course/view.php?id=76”>Moodle</a>.
25.2. 09:00 - 15:00:
MIRA-STAN 1/2 -
Meeting point at the microscope. This is a two-step training, register for part 2 in our booking system. Obligatory prerequisites must be completed 2 days before the training. More information about the training is available on our <a href=”https://cfmoodle.ceitec.vutbr.cz/course/view.php?id=76”>Moodle</a>.
4.3. 13:00 - 16:00:
MIRA-STAN 2/2 -
Meeting point at the microscope. This is a two-step training, register for part 1 in our booking system. More information about the training is available on our <a href=”https://cfmoodle.ceitec.vutbr.cz/course/view.php?id=76”>Moodle</a>.
6.3. 09:00 - 12:00:
MIRA-STAN 2/2 -
Meeting point at the microscope. This is a two-step training, register for part 1 in our booking system. More information about the training is available on our <a href=”https://cfmoodle.ceitec.vutbr.cz/course/view.php?id=76”>Moodle</a>.
Scanning electron microscope (SEM) MIRA3 XMU
Description
• Scanning electron microscope (SEM) is used to study the morphology and topography of conductive and non-conductive materials in high resolution (micro to nano-scale).
• Observation of surface samples with high depth of focus using multiple detection system (SE, BSE, STEM) including elemental analysis using energy dispersive spectrometer (EDS).
Applications
• Observation of both the surface and internal structure of micro and nano-objects (phase interface such as matrix-filler/reinforcement, particle distribution, aggregates and defects, fracture surfaces, porous 3D materials, units of supramolecular structure, etc.)
• evaluation of the shape and dimensions (length, diameter, volume, roughness) of powders, tubes, short fibers
• fast and highly accurate chemical microanalysis and elemental mapping of a sample surface
• qualitative elemental analysis including determination of the distribution of each element
• quantitative analysis of the individual elements in a sample
• The structural analysis of polymeric materials, biopolymers and composites, biomaterials, ceramics, bones, teeth, substrates for tissue engineering, etc.
Specification
• High Brightness Schottky Emitter
• Detectors:
SE, BSE, In-beam SE, In-Beam BSE
LVSTD
STEM detector
EDX analysis
• High-vacuum (≤9x10-3Pa) or low-vacuum mode (7-500 Pa)
• Magnification 25 to 1 000 000x
• Acceleration voltage 200 V to 30 kV
• X-Y-Z 130×130×100mm
• Maximum specimen height: 106 mm
Publications:
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NATARAJAN, S.; ORAL, Ç.; NOVOBILSKÝ, A.; PUMERA, M., 2024: Intelligent Magnetic Microrobots with Fluorescent Internal Memory for Monitoring Intragastric Acidity. ADVANCED FUNCTIONAL MATERIALS 34(29), p. 1 - 12, doi: 10.1002/adfm.202401463; FULL TEXT
(FTIR-CHEMLAB, VERIOS, MIRA-STAN, LEICACOAT-STAN, RIGAKU3) -
HOLÁ, M.; SALAJKOVÁ, Z.; GREGAR, F.; ONDRÁČEK, J.; PAVLIŇÁK, D.; ŠPERKA, P.; HRDLIČKA, A.; KAISER, J.; KANICKÝ, V., 2024: Laser spot overlap in scanning laser ablation ICP-MS analysis: Impact on analytical signal and properties of the generated aerosol. SPECTROCHIMICA ACTA PART B-ATOMIC SPECTROSCOPY 219, doi: 10.1016/j.sab.2024.106999; FULL TEXT
(MIRA-STAN) -
RONOH, K.; NOVOTNÝ, J.; MRŇA, L.; KNÁPEK, A.; SOBOLA, D., 2024: Surface Structuring of the CP Titanium by Ultrafast Laser Pulses. MATERIALS RESEARCH EXPRESS 14(8), p. 1 - 21, doi: 10.3390/app14083164; FULL TEXT
(MIRA-STAN, WITEC-RAMAN, SEE-SYSTEM, DEKTAK) -
KORČUŠKOVÁ, M.; SVATÍK, J.; TOMAL, W.; ŠIKYŇOVÁ, A.; VISHAKHA, V.; PETKO, F.; GSALEK, M.; STALMACH, P.; ORTYL, J.; LEPCIO, P., 2024: Anatase and rutile nanoparticles in photopolymer 3D-printed nanocomposites: Band gap-controlled electron interactions in free-radical and cationic photocuring. REACTIVE & FUNCTIONAL POLYMERS 200, p. 1 - 12, doi: 10.1016/j.reactfunctpolym.2024.105923; FULL TEXT
(WITEC-RAMAN, JASCO, MIRA-STAN, DSC-DISCOVERY) -
Gazdík, R., 2024: Defect localization and analysis in GaN. MASTER´S THESIS , p. 1 - 66; FULL TEXT
(MIRA-STAN, HELIOS, TITAN)
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DRDLÍK, D.; MAŘÁK, V.; HADRABA, H.; CHLUP, Z., 2024: A way for densification of lead-free BaTiO3-based/ZrO2 laminates for energy harvesting applications prepared by electrophoretic deposition. MATERIALS LETTERS 335, doi: 10.1016/j.matlet.2023.135424; FULL TEXT
(MIRA-STAN) -
RONOH, K.; NOVOTNÝ, J.; MRŇA, L.; KNÁPEK, A.; SOBOLA, D., 2024: Analysis of processing efficiency, surface, and bulk chemistry, and nanomechanical properties of the Monel® alloy 400 after ultrashort pulsed laser ablation. MATERIALS RESEARCH EXPRESS 11(1), doi: 10.1088/2053-1591/ad184b; FULL TEXT
(DEKTAK, MIRA-STAN, KRATOS-XPS, NANOINDENTER) -
VALÁŠEK, D.; POUCHLÝ, V.; SALAMON, D., 2024: Turning of high entropy alloy into high entropy carbides by modifying carbon content during reactive sintering. CERAMICS INTERNATIONAL 50(9), p. 15367 - 6, doi: 10.1016/j.ceramint.2024.01.438; FULL TEXT
(MIRA-STAN, RIGAKU3) -
VELIKOV, D.; JANČÍK PROCHÁZKOVÁ, A.; PUMERA, M., 2024: On-the-Fly Monitoring of the Capture and Removal of Nanoplastics with Nanorobots. ACS NANOSCIENCE AU 4(4), p. 243 - 7, doi: 10.1021/acsnanoscienceau.4c00002; FULL TEXT
(MIRA-STAN) -
Escalera-López, D.; Iffelsberger, C.; Zlatar, M.; Novcic, K.; Maselj, N.; Van Pham, C.; Jovanovic, P.; Hodnik, N.; Thiele, S.; Pumera, M.; Cherevko, S. , 2024: Allotrope-dependent activity-stability relationships of molybdenum sulfide hydrogen evolution electrocatalysts. NATURE COMMUNICATIONS 15(1), doi: 10.1038/s41467-024-47524-w; FULL TEXT
(MIRA-STAN, KRATOS-XPS, WITEC-RAMAN) -
Ussia, M.; Urso, M.; Oral, C. M.; Peng, X.; Pumera, M., 2024: Magnetic Microrobot Swarms with Polymeric Hands Catching Bacteria and Microplastics in Water. ACS NANO 18(20), p. 13171 - 13183, doi: 10.1021/acsnano.4c02115; FULL TEXT
(MIRA-STAN) -
Gustafsson, L.; Kvick, M.; Åstrand, C.; Ponsteen, N.; Dorka, N.; Hegrová, V.; Svanberg, S.; Horák, J.; Jansson, R.; Hedhammar, M.; van der Wijngaart, W., 2023: Scalable Production of Monodisperse Bioactive Spider Silk Nanowires. MACROMOLECULAR BIOSCIENCE 23(4), doi: 10.1002/mabi.202200450; FULL TEXT
(MIRA-STAN) -
VISHAKHA, V.; ABDELLATIF, A.; MICHALIČKA, J.; WHITE, P.; LEPCIO, P.; TINOCO NAVARRO, L.; JANČÁŘ, J., 2023: Carboxymethyl starch as a reducing and capping agent in the hydrothermal synthesis of selenium nanostructures for use with three-dimensional-printed hydrogel carriers. ROYAL SOCIETY OPEN SCIENCE 10(10), p. 1 - 17, doi: 10.1098/rsos.230829; FULL TEXT
(ZETASIZER, RIGAKU3, VERIOS, MIRA-STAN, LEICACOAT-STAN, TITAN, FTIR-CHEMLAB, KRATOS-XPS, JASCO) -
PENG, X.; URSO, M.; PUMERA, M., 2023: Metal oxide single-component light-powered micromotors for photocatalytic degradation of nitroaromatic pollutants. NPJ CLEAN WATER 6(6), p. 1 - 7, doi: 10.1038/s41545-023-00235-z; FULL TEXT
(MIRA-STAN, KRATOS-XPS) -
TINOCO NAVARRO, L.; BEDNAŘÍKOVÁ, V.; KAŠTYL, J.; CIHLÁŘ, J., 2023: Structure and Photocatalytic Properties of Ni-, Co-, Cu-, and Fe-Doped TiO2 Aerogels. GELS 9(5), p. 1 - 21, doi: 10.3390/gels9050357; FULL TEXT
(RIGAKU3, VERIOS, BET-ANAMET, JASCO, MIRA-STAN, TITAN) -
JANČÍK PROCHÁZKOVÁ, A.; JAŠEK, V.; FIGALLA, S.; PUMERA, M., 2023: Photocatalytic Microplastics ´On-The-fly´ Degradation via Motile Quantum Materials-Based Microrobots. ADVANCED OPTICAL MATERIALS , p. 1 - 9, doi: 10.1002/adom.202300782; FULL TEXT
(MIRA-STAN, RIGAKU3) -
Vida, J.; Pospisil, J.; Souček, P.; Weiter, M.; Homola, T., 2023: Rapid, low-temperature, air plasma sintering of mesoporous titania electron transporting layers in perovskite solar cells. SOLAR ENERGY MATERIALS AND SOLAR CELLS 263, doi: 10.1016/j.solmat.2023.112562; FULL TEXT
(KRATOS-XPS, MIRA-STAN) -
Bondarev, A.; Simonovic, K.; Vitu, T.; Kožmín, P.; Syrovatka, Š.; Polcar, T., 2023: Textured coating or coated texture: Femtosecond laser texturing of a-C:H/WC coatings for dry friction applications. SURFACE AND COATINGS TECHNOLOGY 469, doi: 10.1016/j.surfcoat.2023.129808; FULL TEXT
(HELIOS, KRATOS-XPS, MIRA-STAN) -
WERT, S.; IFFELSBERGER, C.; KANDAMBATH PADINJAREVEETIL, A.; PUMERA, M., 2023: Edges of Layered FePSe3 Exhibit Increased Electrochemical and Electrocatalytic Activity Compared to Basal Planes. ACS APPLIED ELECTRONIC MATERIALS 5(2), p. 928 - 7, doi: 10.1021/acsaelm.2c01493; FULL TEXT
(RIGAKU3, MIRA-STAN) -
JANČÍK PROCHÁZKOVÁ, A.; PUMERA, M., 2023: Light-powered swarming phoretic antimony chalcogenide-based microrobots with ´on-the-fly´ photodegradation abilities. NANOSCALE 15(12), p. 5726 - 9, doi: 10.1039/d3nr00098b; FULL TEXT
(MIRA-STAN, RIGAKU3) -
JAQUES, V.; HOLCOVÁ, K., 2023: Calcareous nannofossil assemblage in paintings chalk ground for provenance analysis: three original paintings compared to european source materials. HERITAGE SCIENCE 11(1), p. 1 - 11, doi: 10.1186/s40494-023-00974-9; FULL TEXT
(MIRA-STAN) -
ŠKARPA, P.; JANČÁŘ, J.; LEPCIO, P.; ANTOŠOVSKÝ, J.; KLOFÁČ, D.; KRIŠKA, T.; ABDELLATIF, A.; BRTNICKÝ, M., 2023: Effect of fertilizers enriched with bio-based carriers on selected growth parameters, grain yield and grain quality of maize (Zea mays L.) . EUROPEAN JOURNAL OF AGRONOMY 143, doi: 10.1016/j.eja.2022.126714; FULL TEXT
(FTIR-CHEMLAB, MIRA-STAN) -
SEVRIUGINA, V.; PAVLIŇÁK, D.; ONDREÁŠ, F.; JAŠEK, O.; ŠTAFFOVÁ, M.; LEPCIO, P., 2023: Matching Low Viscosity with Enhanced Conductivity in Vat Photopolymerization 3D Printing: Disparity in the Electric and Rheological Percolation Thresholds of Carbon-Based Nanofillers Is Controlled by the Matrix Type and Filler Dispersion. ACS OMEGA 8(48), p. 45566 - 12, doi: 10.1021/acsomega.3c05683; FULL TEXT
(KRATOS-XPS, WITEC-RAMAN, BET-DEGASSER, MIRA-STAN, FTIR-CHEMLAB, LEICACOAT-STAN) -
GHOSH, K.; IFFELSBERGER, C.; KONEČNÝ, M.; VYSKOČIL, J.; MICHALIČKA, J.; PUMERA, M., 2023: Nanoarchitectonics of Triboelectric Nanogenerator for Conversion of Abundant Mechanical Energy to Green Hydrogen. ADVANCED ENERGY MATERIALS 13(11), doi: 10.1002/aenm.202203476; FULL TEXT
(VERIOS, MIRA-STAN, TITAN, RIGAKU3, MPS150, KEITHLEY-4200, ICON-SPM) -
Jancik-Prochazkova, A.; Michalkova, H.; Heger, Z.; Pumera, M., 2023: Hydrogen Bonding Nanoarchitectonics of Organic Pigment-Based Janus Microrobots with Entering Capability into Cancer Cells. ACS NANO 17(1), p. 146 - 156, doi: 10.1021/acsnano.2c05585; FULL TEXT
(VERIOS, MIRA-STAN, LEICACOAT-STAN, FTIR) -
DEÁK, A.; SZABÓ, P.; BEDNAŘÍKOVÁ, V.; CIHLÁŘ, J.; DEMETER, A.; REMEŠOVÁ, M.; COLACINO, E.; ČELKO, L., 2023: The first solid-state route to luminescent Au(I)-glutathionate and its pH-controlled transformation into ultrasmall oligomeric Au10-12(SG)10-12 nanoclusters for application in cancer radiotheraphy. FRONTIERS IN CHEMISTRY 11, doi: 10.3389/fchem.2023.1178225; FULL TEXT
(RIGAKU3, KRATOS-XPS, MIRA-STAN, VERIOS, LEICACOAT-STAN) -
Žůrek, M., 2023: Butyl Rubber Modified Using Expanded Graphite. MASTER´S THESIS ; FULL TEXT
(MIRA-STAN) -
USSIA, M.; URSO, M.; KRATOCHVÍLOVÁ, M.; NAVRÁTIL, J.; BALVAN, J.; MAYORGA-MARTINEZ, C.; VYSKOČIL, J.; MASAŘÍK, M.; PUMERA, M., 2023: Magnetically Driven Self-Degrading Zinc-Containing Cystine Microrobots for Treatment of Prostate Cancer. SMALL 19(17), doi: 10.1002/smll.202208259; FULL TEXT
(MIRA-STAN) -
UKROPCOVÁ, I.; DAO, R.; ŠTUBIAN, M.; KOLÍBAL, M.; ŠIKOLA, T.; WILLINGER, M.; WANG, Z.; ZLÁMAL, J.; BÁBOR, P., 2023: Electron Tractor Beam: Deterministic Manipulation of Liquid Droplets on Solid Surfaces. ADVANCED MATERIALS INTERFACES 10(2), doi: 10.1002/admi.202201963; FULL TEXT
(NANOSAM, LITESCOPE-LYRA, MIRA-STAN) -
Novotný, K., 2023: Composite materials with enhanced coefficient of linear attenuation of ionizing radiation. MASTER´S THESIS ; FULL TEXT
(MIRA-STAN) -
SANNA, M.; NOVCIC, K.; NG, S.; ČERNÝ, M.; PUMERA, M., 2023: The unexpected photoelectrochemical activity of MAX phases: the role of oxide impurities. JOURNAL OF MATERIALS CHEMISTRY A 11(6), p. 3080 - 11, doi: 10.1039/d2ta06929f; FULL TEXT
(MIRA-STAN, KRATOS-XPS, RIGAKU3) -
SLÁMEČKA, K.; KASHIMBETOVA, A.; POKLUDA, J.; ZIKMUND, T.; KAISER, J.; MONTUFAR JIMENEZ, E.; ČELKO, L., 2023: Fatigue behaviour of titanium scaffolds with hierarchical porosity produced by material extrusion additive manufacturing. MATERIALS & DESIGN 225, p. 1 - 11, doi: 10.1016/j.matdes.2022.111453; FULL TEXT
(MIRA-STAN, micro-CT-L240, RIGAKU3) -
SEDLÁŘ, M.; VERČIMÁKOVÁ, K.; FOHLEROVÁ, Z.; IZSÁK, D.; CHALUPOVÁ, M.; SUCHÝ, P.; DOHNALOVÁ, M.; SOPUCH, T.; VOJTOVÁ, L., 2023: A synergistic effect of fibrous carboxymethyl cellulose with equine collagen improved the hemostatic properties of freeze-dried wound dressings. CELLULOSE , p. 1 - 19, doi: 10.1007/s10570-023-05571-4; FULL TEXT
(LEICACOAT-STAN, MIRA-STAN) -
RYŠAVÁ, L.; DVOŘÁK, M.; VOJTOVÁ, L.; DORAZILOVÁ, J.; SEDLÁČEK, P.; KUBÁŇ, P., 2023: Fully soluble polymeric foams for in-vial dried blood spot collection and analysis of acidic drugs by capillary electrophoresis. ANALYTICA CHIMICA ACTA 1241, doi: 10.1016/j.aca.2023.340793; FULL TEXT
(MIRA-STAN) -
KACVINSKÁ, K.; PAVLIŇÁKOVÁ, V.; POLÁČEK, P.; MICHLOVSKÁ, L.; HEFKA BLAHNOVÁ, V.; FILOVÁ, E.; KNOZ, M.; LIPOVÝ, B.; HOLOUBEK, J.; FALDYNA, M.; PAVLOVSKÝ, Z.; VÍCENOVÁ, M.; CVANOVÁ, M.; JARKOVSKÝ, J.; VOJTOVÁ, L., 2023: Accelular nanofbrous bilayer scafold intrapenetrated with polydopamine network and implemented into a full-thickness wound of a white-pig model afects infammation and healing process. JOURNAL OF NANOBIOTECHNOLOGY 21(1), p. 1 - 24, doi: 10.1186/s12951-023-01822-5; FULL TEXT
(MIRA-STAN) -
ORAL, Ç.; USSIA, M.; URSO, M.; SALÁT, J.; NOVOBILSKÝ, A.; ŠTEFÁNIK, M.; RŮŽEK, D.; PUMERA, M., 2023: Radiopaque Nanorobots as Magnetically Navigable Contrast Agents for Localized In Vivo Imaging of the Gastrointestinal Tract. ADVANCED HEALTHCARE MATERIALS 12(8), doi: 10.1002/adhm.202202682; FULL TEXT
(VERIOS, MIRA-STAN, RIGAKU3, VERSALAB) -
MILOSAVLJEVIĆ, V.; KOŠARIŠŤANOVÁ, L.; DOLEŽELÍKOVÁ, K.; ADAM, V.; PUMERA, M., 2022: Microrobots with Antimicrobial Peptide Nanoarchitectonics for the Eradication of Antibiotic-Resistant Biofilms. ADVANCED MATERIALS FOR OPTICS AND ELECTRONICS 32(43), p. 1 - 11, doi: 10.1002/adfm.202112935; FULL TEXT
(LEICACOAT-NANO, MIRA-EBL, MIRA-STAN, KRATOS-XPS) -
KANDAMBATH PADINJAREVEETIL, A.; ALDUHAISH, O.; ADIL, S.; PUMERA, M., 2022: Grafting of Pd on Covalently and Noncovalently Modified N-Doped Graphene for Electrocatalysis. ADVANCED MATERIALS INTERFACES 9(27), p. 2102317 - 8, doi: 10.1002/admi.202102317; FULL TEXT
(MIRA-STAN, KRATOS-XPS, LYRA) -
MUNOZ MARTIN, J.; URSO, M.; PUMERA, M., 2022: Self-Propelled Multifunctional Microrobots Harboring Chiral Supramolecular Selectors for ´Enantiorecogniton-on-the-Fly´. ANGEWANDTE CHEMIE-INTERNATIONAL EDITION 61(14), p. 1 - 7, doi: 10.1002/anie.202116090; FULL TEXT
(MIRA-STAN, VERSALAB) -
ŘÍHOVÁ, M.; LEPCIO, P.; ČIČMANCOVÁ, V.; FRUMAROVÁ, B.; HROMÁDKO, L.; BUREŠ, F.; VOJTOVÁ, L.; MACÁK, J., 2022: The centrifugal spinning of vitamin doped natural gum fibers for skin regeneration. CARBOHYDRATE POLYMERS (ELECTRONIC) 294, p. 1 - 10, doi: 10.1016/j.carbpol.2022.119792; FULL TEXT
(MIRA-STAN, FTIR-CHEMLAB, LEICACOAT-STAN, IR-RAMAN) -
MAYORGA BURREZO, P.; MAYORGA-MARTINEZ, C.; PUMERA, M., 2022: Light-Driven Micromotors to Dissociate Protein Aggregates That Cause Neurodegenerative Diseases. ADVANCED FUNCTIONAL MATERIALS , p. 2106699-1 - 8, doi: 10.1002/adfm.202106699; FULL TEXT
(MIRA-STAN, RIGAKU9, KRATOS-XPS) -
URSO, M.; USSIA, M.; NOVOTNÝ, F.; PUMERA, M., 2022: Trapping and detecting nanoplastics by MXene-derived oxide microrobots. NATURE COMMUNICATIONS 13(1), p. 3573-1 - 14, doi: 10.1038/s41467-022-31161-2; FULL TEXT
(LEICACOAT-NANO, MIRA-STAN, RIGAKU9, KRATOS-XPS, VERSALAB) -
IFFELSBERGER, C.; ROJAS TIZÓN, J.; PUMERA, M., 2022: Photo-Responsive Doped 3D-Printed Copper Electrodes for Water Splitting: Refractory One-Pot Doping Dramatically Enhances the Performance. JOURNAL OF PHYSICAL CHEMISTRY C (WEB) 126(21), p. 9016 - 11, doi: 10.1021/acs.jpcc.1c10686; FULL TEXT
(TEGRAMIN, MIRA-STAN, RIGAKU3, KRATOS-XPS) -
Čermák, A.; Simonović, K.; Bondarev, A.; Kožmín, P.; Syrovátka, Š.; Polcar, T.; Syrovátka, J., 2022: Femtosecond laser texturing of DLC-based coatings by DLW method with sub-micrometer precision. THE INTERNATIONAL JOURNAL OF ADVANCED MANUFACTURING TECHNOLOGY 121(11-12), p. 8479 - 8494, doi: 10.1007/s00170-022-09855-0; FULL TEXT
(MIRA-STAN, KRATOS-XPS) -
KORČUŠKOVÁ, M.; SEVRIUGINA, V.; ONDREÁŠ, F.; SVATÍK, J.; TOMAL, W.; VISHAKHA, V.; ORTYL, J.; LEPCIO, P., 2022: Photoactivity, conversion kinetics, nanoreinforcement, post-curing, and electric/dielectric properties of functional 3D printable photopolymer resin filled with bare and alumina-doped ZnO nanoparticles. POLYMER TESTING 116, p. 1 - 10, doi: 10.1016/j.polymertesting.2022.107798; FULL TEXT
(MIRA-STAN, FTIR-CHEMLAB, RIGAKU9) -
LEPCIO, P.; SVATÍK, J.; REŽNÁKOVÁ, E.; ZICHA, D.; LESSER, A.; ONDREÁŠ, F., 2022: Anisotropic solid-state PLA foaming templated by crystal phase pre-oriented with 3D printing: cell supporting structures with directional capillary transfer function. JOURNAL OF MATERIALS CHEMISTRY B 10(15), p. 2889 - 10, doi: 10.1039/d1tb02133h; FULL TEXT
(MIRA-STAN, FTIR-CHEMLAB, LEICACOAT-STAN) -
USSIA, M.; URSO, M.; KMENT, Š.; FIALOVÁ, T.; KLÍMA, K.; DOLEŽELÍKOVÁ, K.; PUMERA, M., 2022: Light-Propelled Nanorobots for Facial Titanium Implants Biofilms Removal. SMALL 18(22), p. 1 - 10, doi: 10.1002/smll.202200708; FULL TEXT
(MIRA-STAN, LEICACOAT-STAN) -
IFFELSBERGER, C.; NG, S.; PUMERA, M., 2022: Photoelectrolysis of TiO2 is highly localized and the selectivity is affected by the light. CHEMICAL ENGINEERING JOURNAL 446, p. 136995-1 - 12, doi: 10.1016/j.cej.2022.136995; FULL TEXT
(WITEC-RAMAN, VERIOS, MIRA-STAN, RIGAKU3, KRATOS-XPS) -
Breuer, JP.; Galgoczi, G.; Fioretti, V.; Zlamal, J.; Liska, P.; Werner, N.; Santin, G.; Boudin, N.; Ferreira, I. ; Guainazzi, M.; von Kienlin, A. ; Lotti, S.; Mineo, T.; Molendi, S.; Perinati, E., 2022: Athena charged particle diverter simulations: effects of micro-roughness on proton scattering using Geant4. SPACE TELESCOPES AND INSTRUMENTATION 2022: ULTRAVIOLET TO GAMMA RAY , doi: 10.1117/12.2630076; FULL TEXT
(MIRA-STAN, ICON-SPM) -
WERT, S.; IFFELSBERGER, C.; NOVCIC, K.; PUMERA, M., 2022: Corrosion of catalyst in high resolution: Layered transition metal dichalcogenides electrocatalyse water splitting and corrode during the process. JOURNAL OF CATALYSIS 416, p. 85 - 7, doi: 10.1016/j.jcat.2022.10.023; FULL TEXT
(MIRA-STAN, KRATOS-XPS, RIGAKU3) -
Jancik-Prochazkova, A.; Mayorga-Martinez, C. C.; Vyskočil, J.; Pumera, M., 2022: Swarming Magnetically Navigated Indigo-Based Hydrophobic Microrobots for Oil Removal. ACS APPLIED MATERIALS & INTERFACES 14(40), p. 45545 - 45552, doi: 10.1021/acsami.2c09527; FULL TEXT
(LEICACOAT-NANO, MIRA-STAN, FTIR) -
LEPCIO, P.; SVATÍK, J.; ŠTAFFOVÁ, M.; LESSER, A.; ONDREÁŠ, F., 2022: Revealing the Combined Nanoconfinement Effect by Soft and Stiff Inclusions in PMMA/Silica CO2 Blown Foams. MACROMOLECULAR MATERIALS AND ENGINEERING 307(11), p. 1 - 9, doi: 10.1002/mame.202200403; FULL TEXT
(MIRA-STAN, LEICACOAT-STAN, FTIR-CHEMLAB) -
BÁČOVÁ, J.; HROMÁDKO, L.; NÝVLTOVÁ, P.; BRŮČKOVÁ, L.; MOTOLA, M.; BULÁNEK, R.; ŘÍHOVÁ, M.; ROUŠAR, T.; MACÁK, J., 2022: Ceramic fibers do not exhibit larger toxicity in pulmonary epithelial cells than nanoparticles of the same chemical composition. ENVIRONMENTAL SCIENCE: NANO 9(12), p. 4484 - 13, doi: 10.1039/d2en00217e; FULL TEXT
(MIRA-STAN) -
MUNOZ MARTIN, J.; ROJAS TIZÓN, J.; PUMERA, M., 2022: Faceted Crystal Nanoarchitectonics of Organic-Inorganic 3D-Printed Visible-Light Photocatalysts. ACS APPLIED ENERGY MATERIALS 5(3), p. 3252 - 7, doi: 10.1021/acsaem.1c03863; FULL TEXT
(MIRA-STAN, KRATOS-XPS) -
PENG, X.; URSO, M.; USSIA, M.; PUMERA, M., 2022: Shape-Controlled Self-Assembly of Light-Powered Microrobots into Ordered Microchains for Cells Transport and Water Remediation. ACS NANO 16(5), p. 7615 - 11, doi: 10.1021/acsnano.1c11136; FULL TEXT
(MIRA-STAN, RIGAKU3) -
GAO, W.; MICHALIČKA, J.; PUMERA, M., 2022: Hierarchical Atomic Layer Deposited V2O5 on 3D Printed Nanocarbon Electrodes for High-Performance Aqueous Zinc-Ion Batteries. SMALL 18(1), p. 2105572-1 - 13, doi: 10.1002/smll.202105572; FULL TEXT
(ALD, VERIOS, MIRA-STAN, TITAN, RIGAKU3, KRATOS-XPS) -
TESAŘ, J.; MUNOZ MARTIN, J.; PUMERA, M., 2022: Limitations and Benefits of MAX Phases in Electroanalysis. ELECTROANALYSIS 33, p. 56 - 5, doi: 10.1002/elan.202100473; FULL TEXT
(MIRA-STAN) -
Bondarev, A.; Ponomarev, I.; Muydinov, R.; Polcar, T., 2022: Friend or Foe? Revising the Role of Oxygen in the Tribological Performance of Solid Lubricant MoS2. ACS APPLIED MATERIALS AND INTERFACES 14(49), p. 55051 - 55061, doi: 10.1021/acsami.2c15706; FULL TEXT
(HELIOS, TITAN, KRATOS-XPS, VERIOS, MIRA-STAN) -
JAQUES, V.; ZIKMUNDOVÁ, E.; HOLAS, J.; ZIKMUND, T.; KAISER, J.; HOLCOVÁ, K., 2022: Cyclododecane shaping, sublimation rate and residue analysis for the extraction of painting micro-samples from resin cross-sections. SCIENTIFIC REPORTS 12(1), p. 1 - 11, doi: 10.1038/s41598-022-22448-x; FULL TEXT
(LEICACOAT-STAN, MIRA-STAN, CITOVAC, TEGRAMIN) -
MUNOZ MARTIN, J.; IFFELSBERGER, C.; REDONDO NEGRETE, E.; PUMERA, M., 2022: Design of bimetallic 3D-printed electrocatalysts via galvanic replacement to enhance energy conversion systems. APPLIED CATALYSIS B: ENVIRONMENTAL 316, p. 1 - 9, doi: 10.1016/j.apcatb.2022.121609; FULL TEXT
(TEGRAMIN, CITOVAC, MIRA-STAN, KRATOS-XPS, RIGAKU9) -
WERT, S.; IFFELSBERGER, C.; NOVCIC, K.; MATYSIK, F.; PUMERA, M., 2022: Edges are more electroactive than basal planes in synthetic bulk crystals of TiS2 and TiSe2. APPLIED MATERIALS TODAY 26, p. 101309-1 - 7, doi: 10.1016/j.apmt.2021.101309; FULL TEXT
(MIRA-STAN, KRATOS-XPS, ICON-SPM) -
JAQUES, V.; ZIKMUNDOVÁ, E.; HOLAS, J.; ZIKMUND, T.; KAISER, J.; HOLCOVÁ, K., 2022: Conductive cross-section preparation of non-conductive painting micro-samples for SEM analysis. SCIENTIFIC REPORTS 12(1), doi: 10.1038/s41598-022-21882-1; FULL TEXT
(MIRA-STAN, CITOPRESS, LEICACOAT-STAN, TEGRAMIN) -
PENG, X.; URSO, M.; BALVAN, J.; MASAŘÍK, M.; PUMERA, M., 2022: Self-Propelled Magnetic Dendrite-Shaped Microrobots for Photodynamic Prostate Cancer Therapy. ANGEWANDTE CHEMIE-INTERNATIONAL EDITION 61(48), doi: 10.1002/anie.202213505; FULL TEXT
(MIRA-STAN, RIGAKU3, KRATOS-XPS) -
ŠTAFFOVÁ, M.; ONDREÁŠ, F.; SVATÍK, J.; ZBONČÁK, M.; JANČÁŘ, J.; LEPCIO, P., 2022: 3D printing and post-curing optimization of photopolymerized structures: Basic concepts and effective tools for improved thermomechanical properties. POLYMER TESTING 108, p. 1 - 11, doi: 10.1016/j.polymertesting.2022.107499; FULL TEXT
(FTIR-CHEMLAB, MIRA-STAN, LEICACOAT-STAN, LEXT) -
ORAL, Ç.; USSIA, M.; YAVUZ, D.; PUMERA, M., 2022: Shape Engineering of TiO2 Microrobots for ´On-the-Fly´ Optical Brake. SMALL 18(10), p. 21076271-6 - 6, doi: 10.1002/smll.202106271; FULL TEXT
(LEICACOAT-STAN, VERIOS, MIRA-STAN, RIGAKU3) -
NOVCIC, K.; IFFELSBERGER, C.; PUMERA, M., 2022: Layered MAX phase electrocatalyst activity is driven by only a few hot spots. JOURNAL OF MATERIALS CHEMISTRY A , p. 3206 - 10, doi: 10.1039/d1ta06419c; FULL TEXT
(RIGAKU9, MIRA-STAN, LEICACOAT-STAN, ICON-SPM) -
SVATÍK, J.; LEPCIO, P.; ONDREÁŠ, F.; ZÁRYBNICKÁ, K.; ZBONČÁK, M.; MENČÍK, P.; JANČÁŘ, J., 2021: PLA toughening via bamboo-inspired 3D printed structural design. POLYMER TESTING 104, p. 1 - 9, doi: 10.1016/j.polymertesting.2021.107405; FULL TEXT
(MIRA-STAN) -
URSO, M.; USSIA, M.; PUMERA, M., 2021: Breaking Polymer Chains with Self-Propelled Light-Controlled Navigable Hematite Microrobots. ADVANCED FUNCTIONAL MATERIALS 31(28), p. 2101510-1 - 10, doi: 10.1002/adfm.202101510; FULL TEXT
(MIRA-STAN, KRATOS-XPS, RIGAKU9) -
MANAKHOV, A.; SITNIKOVA, N.; TSYGANKOVA, A.; ALEKSEEV, A.; ADAMENKO, L.; PERMYAKOVA, E.; BAIDYSHEV, V.; POPOV, Z.; BLAHOVÁ, L.; ELIÁŠ, M.; ZAJÍČKOVÁ, L.; SOLOVIEVA, A., 2021: Electrospun Biodegradable Nanofibers Coated Homogenously by Cu Magnetron Sputtering Exhibit Fast Ion Release. Computational and Experimental Study. MEMBRANES 11(12), p. 1 - 19, doi: 10.3390/membranes11120965; FULL TEXT
(MAGNETRON, KRATOS-XPS, MIRA-STAN) -
PENG, X.; URSO, M.; PUMERA, M., 2021: Photo-Fenton Degradation of Nitroaromatic Explosives by Light-Powered Hematite Microrobots: When Higher Speed Is Not What We Go For. SMALL METHODS 5(10), p. 2100617-1 - 9, doi: 10.1002/smtd.202100617; FULL TEXT
(MIRA-STAN, CRYOGENIC) -
ORAL, Ç.; USSIA, M.; PUMERA, M., 2021: Self-Propelled Activated Carbon Micromotors for ´On-the-Fly´ Capture of Nitroaromatic Explosives. JOURNAL OF PHYSICAL CHEMISTRY C (PRINT) 125(32), p. 18040 - 6, doi: 10.1021/acs.jpcc.1c05136; FULL TEXT
(MIRA-STAN) -
TOMAL, W.; KROK, D.; CHACHAJ-BRESKIESZ, A.; LEPCIO, P.; ORTYL, J., 2021: Harnessing light to create functional, three-dimensional polymeric materials: multitasking initiation systems as the critical key to success. ADDITIVE MANUFACTURING 48, p. 1 - 15, doi: 10.1016/j.addma.2021.102447; FULL TEXT
(MIRA-STAN) -
IFFELSBERGER, C.; PUMERA, M., 2021: High resolution electrochemical additive manufacturing of microstructured active materials: case study of MoSx as a catalyst for the hydrogen evolution reaction. JOURNAL OF MATERIALS CHEMISTRY A 9(38), p. 22072 - 10, doi: 10.1039/d1ta05581j; FULL TEXT
(MIRA-STAN, VERIOS, KRATOS-XPS, LYRA) -
LEPCIO, P.; ONDREÁŠ, F.; ZÁRYBNICKÁ, K.; ZBONČÁK, M.; SVATÍK, J.; JANČÁŘ, J., 2021: Phase diagram of bare particles in polymer nanocomposites: Uniting solution and melt blending. POLYMER 230, p. 124033 - 6, doi: 10.1016/j.polymer.2021.124033; FULL TEXT
(MIRA-STAN, VERIOS) -
NOVOTNÁ, V., HORÁK, J., KONEČNÝ, M., HEGROVÁ, V., NOVOTNÝ, O., NOVÁČEK, Z., NEUMAN, J., 2020: AFM-in-SEM as a Tool for Comprehensive Sample Surface Analysis. MICROSCOPY TODAY , p. 38 - 9, doi: 10.1017/S1551929520000875; FULL TEXT
(MIRA-STAN, LITESCOPE-LYRA) -
ZBONČÁK, M.; ONDREÁŠ, F.; UHLÍŘ, V.; LEPCIO, P.; MICHALIČKA, J.; JANČÁŘ, J., 2020: Translation of segment scale stiffening into macro scale reinforcement in polymer nanocomposites. POLYMER ENGINEERING AND SCIENCE 60(3), p. 587 - 10, doi: 10.1002/pen.25317; FULL TEXT
(MIRA-STAN, FISCHIONE-TEM-MILL, CRYOGENIC)
Photogallery
Specification
Type | MIRA3 | |
---|---|---|
Manufacturer | TESCAN | |
Type of microscope | SEM | |
Electron beam source | Schottky FEG cathode | |
Acceleration voltage | 200 eV – 30 kV 50 eV – 30 kV for Beam Deceleration Mode | |
Electron beam current | 2 pA – 200 nA | |
Magnification | max 1 000 000 x | |
View Field | 6,4 mm at WD 10 mm | |
Detectors | SE Low energy BSE In-Beam SE In-Beam BSE STEM (transmission mode) s BF, DF LVSTD (detector SE v Low-vacuum mode) | |
Resolution in High-vacuum mode | SE In-Beam SE | 1.2 nm at 30 kV 2.5 nm at 3.0 kV 1.0 nm at 30 kV 1.5 nm at 3.0 kV 2.5 nm at 200 V 0.8 nm at 30 kV |
Resolution in Low-vacuum mode | BSE LVSTD | 2.0 nm at 30 kV 1.5 nm at 30 kV |
Detector EDX | X-max20 Surface of SDD chipset 20 mm2 <127eV @ Mn Kα Oxford Instruments | |
Observation modes | Resolution, Depth, Field, Wide field, Channeling | |
Additional imaging modes | Beam Deceleration Mode (BDM) | |
Stage | Standard TESCAN stage X, Y = 130 mm (od -65 do +65 mm) Z = 100 mm Tilt from -30° to +90° Rotation 360° +TESCAN STEM sample holder (8 samples – standard TEM grids) | |
Peltier stage | Diameter of the specimen holder: | 12.5 mm |
Temperature range: | -50 °C to +70 °C (High Vacuum Mode) | |
Cooling speed: | 30 °C/min | |
Temperature accuracy: | ±1.2 °C | |
Temperature stability: | ±0.2 °C | |
Chamber | Chamber XM Width 290 mm x Depth 340 mm IR navigation camera | |
Vacuum | High-vacuum mode <9·10-3 Pa Low-vacuum mode 7–500 Pa Electron gun pressure <3·10-7 Pa |