Electrolytical polisher Lectropol 5 (LECTROPOL)
Guarantor:
Jiří Holas
Instrument status:
Operational, 3.9.2021 10:21
Equipment placement:
CEITEC Nano - A1.04
Machine for automatic micro-processor controlled electrolytical polishing and etching of metallographic specimens. Lectropol 5 is equipped with a scanning function, i.e. a predefined voltage range is scanned to determine the current density curve. This curve is used to define the correct voltage for polishing and etching. The machine features database with methods for various types of materials. LectroPol-5 is equipped with a built-in measuring and control system, constantly monitoring the electrolyte temperature. The inseparable part of the instrument setup is a recirculating chiller Lauda RP 870, capable of providing electrolyte temperature down to –20 °C.
The sample surface to be polished is exposed to electrolyte through an opening in a mask (standard operation) or by immersion into it in a stainless steel dish (external etching cell).
Publications:
-
Šmíd, M.; Koutný, D.; Neumannová, K.; Chlup, Z.; Náhlík, L.; Jambor, M., 2023: Cyclic behaviour and microstructural evolution of metastable austenitic stainless steel 304L produced by laser powder bed fusion. ADDITIVE MANUFACTURING 68, doi: 10.1016/j.addma.2023.103503; FULL TEXT
(LYRA, TITAN, LECTROPOL) -
ŠIMONOVÁ, L.; MATĚJKA, M.; KNÁPEK, A.; KRÁLÍK, T.; POKORNÁ, Z.; MIKA, F.; FOŘT, T.; MAN, O.; ŠKARVADA, P.; OTÁHAL, A.; ČUDEK, P., 2021: Nanostructures for Achieving Selective Properties of a Thermophotovoltaic Emitter. NANOMATERIALS 11(9), p. 1 - 14, doi: 10.3390/nano11092443; FULL TEXT
(LECTROPOL)
Photogallery
Specification
Output voltage/current
Regime | Voltage | Current |
---|---|---|
Polishing | 0–120V | (1V steps) / 6A |
Etching | 0–25V | (0.5V steps) / 6A |
External Etching | 0–15V | (0.5V steps) / 1.5A |
Software and electronics
Display | 128 × 240 dots (16 × 40 characters) |
---|---|
Controls | touch pad |
Database | 10 built-in Struers methods + 20 user definable methods |
Standard consumables
Electrolyte | Applicable to: |
---|---|
A2 | Aluminium |
Iron | |
Nickel | |
Silver | |
Stainless Steel | |
Steel | |
Tin | |
Titanium | |
D2 | copper, copper alloys |
Other electrolytes shall only be brought in after approval!
Mask opening | Area: |
---|---|
round | 0.5 cm2 |
1 cm2 | |
rectangular | 2 cm2 |
5 cm2 |
Custom shaped openings can be manufactured using a blind mask.
Documents
Here is place for your documents.