LVEM 25E (LVEM)


Guarantor:
Eva Kolíbalová, Ph.D.

Instrument status:
Operational Operational

Equipment placement:
CEITEC Nano - A1.11

Upcoming trainings:
15.1. 09:00 - 16:00: LVEM-training -
29.1. 09:00 - 15.1. 16:00: LVEM-training -
22.1. 09:00 - 15:00: LVEM-training -


The LVEM 25E (Low Voltage Electron Microscope) is a versatile and easy-to-use FEG-type transmission electron microscope (TEM) that combines several imaging modes: transmission mode, electron diffraction mode, scanning transmission mode, and SEM-like scanning mode (BSE detector only), providing the nanometer level resolution. The microscope is also equipped with energy dispersive X-ray spectrometer (EDS) for elemental analysis. It is designed to measure conventionally prepared TEM samples, especially those of low contrast and low atomic number materials (organic matter, polymers). Samples can be thin sections, thin foils, or fine particles dispersed on a standard supporting TEM grid with a diameter of 3.05 mm. High contrast of the light elements is achieved using significantly lower electron energy (25 kV) compared to standard TEM (60-300 kV). Considering this, the sample must be sufficiently thin to image objects containing heavy elements. The maximum thickness of the sample has to be up to 120 nm for low Z samples, ca 20 nm for metals for TEM mode, and up to 200 nm for low Z samples for STEM mode.

Photogallery

Specification

Basic characteristics
   Electron gunSchottky FEG
   Objective lensPermanent magnet
   Projective lensElectrostatic
   Imaging modesTEM, STEM, Electron diffraction, SEM
   Specimen sizeStandard ø 3.05 mm TEM grids
   Specimen movementX, Y: ± 1 mm; Z: ± 0.5 mm
   Specimen (holder) tilt± 20° (manual)

 

Imaging modes
 
TEM
Nominal accelerating voltage25 kV
Resolution1.0 nm
Field of view100 – 0.25 µm
Field of view in Low mag regime225 µm
Electron Diffraction
Nominal accelerating voltage25 kV
STEM
Nominal accelerating voltage10 kV15 kV
Resolution1.0 nm1.3 nm
Maximum field of view105 µm80 µm
SEM (BSE detector)
Nominal accelerating voltage15 kV
Resolution4 nm
Maximum field of view80 µm


Analytical detector specifications

EDS
   Detector typeBruker SDD
   Detector active area30 mm2
   X-Ray windowWindowless
   Energy ResolutionMn Kα ≤ 129 eV

 

Documents

Here is place for your documents.