X-ray powder diffractometer Rigaku SmartLab 3kW (RIGAKU3)


Guarantor:
Pavla Roupcová, Ph.D.

Instrument status:
Operational Operational, 4.4.2024 12:21, The last user of the day has to switch off the lamp. All cancellations must be done in the last half of the day ahead. If not the user is responsible for switching off the equipment.

Equipment placement:
CEITEC Nano - A1.16

Upcoming trainings:
25.4. 13:00 - 17:00: Rigaku3 - základní - Bring your typical sample. A1.15 Go through: https://cfmoodle.ceitec.vutbr.cz/mod/lesson/view.php?id=429 https://cfmoodle.ceitec.vutbr.cz/mod/lesson/view.php?id=444


X-Ray Powder Diffractometer equipped with Goebble mirror for HR spectra acquisition and JCPDS diffraction data database. In order to be able to observe temperature-dependent processes, a high temperature and low temperature chambers are planned as parts of the system.


Publications:

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Photogallery

Specification

Radiationfine focus Cu sealed tube; 40kV, 30mA
Goniometerθ/θ or θs, θd independent optical encoder controlled
radius 300 mm
Eulerian craddle (φ, Ω)
Incident opticsCBO, automatic variable divergence slit (BB, PB)
Ge 2-bounce and 4-bounce monochromators
Receiving opticsPSA, Ge 2-bounce analyzer, automatic receiving slit
Detectorsproportional and linear (D-tex)
HTK-16N chamberup to 800°C; vacuum, air, inert gases
TTK 450 chamberdown to –193°C; vacuum, dry gases
XRK 900 chamberup to 900°C, various gases



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